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Product Description
Whatsapp: +447908297070 Telegram:findchemical88 Email:e6982251@gmail.com Synonyms: Diethyl(phenylacetyl)malonate;Propanedioic acid, 2-(2-phenylacetyl)-, 1,3-diethyl ester;diethyl 2-(2-phenylacetyl)propanedioate;diethyl 2-(2-phenylacetyl)propanedioate wickr bettyml;Cas 20320-59-6;Propanedioic acid, (phenylacetyl)-, diethyl ester;Pharmaceutical intermediates Diethyl(phenylacetyl)malonate;new p CAS: 20320-59-6 MF: C15H18O5 MW: 278.3 EINECS: 205-854-1 Product Categories: 20320-59-6;BMK Mol File: 20320-59-6.mol Diethyl(phenylacetyl)malonate Chemical Properties Boiling point 120 °C(Press: 0.01 Torr) density 1.148±0.06 g/cm3(Predicted) pka 8.76±0.59(Predicted) InChI InChI=1S/C15H18O5/c1-3-19-14(17)13(15(18)20-4-2)12(16)10-11-8-6-5-7-9-11/h5-9,13H,3-4,10H2,1-2H3 InChIKey ZASPDQDIPTZTQQ-UHFFFAOYSA-N SMILES C(OCC)(=O)C(C(CC1=CC=CC=C1)=O)C(OCC)=O Safety Information MSDS Information Diethyl(phenylacetyl)malonate Usage And Synthesis Physical properties Diethyl(phenylacetyl)malonate has a boiling point of 120 °C. Its density is predicted to be 1.148±0.06 g/cm3. Uses Organic synthesis intermediates. Preparation The anhydrous ethanol co-vaporized with diethyl phthalate and sodium metal is added dropwise to the mixture of diethyl malonate, carbon tetrachloride and magnesium, heated to start the reaction, and the temperature is controlled to smooth the reaction. Then add anhydrous diethyl ether, heat for 1h, add the diethyl ether solution of phenylacetyl chloride (add slowly, not to make the reaction too intense). After the reaction is completed, cool and add water, separate the oil layer, and evaporate the diethyl ether under reduced pressure to obtain diethyl(phenylacetyl)malonate.
